Journal of Prevention and Treatment for Stomatological Diseases ›› 2021, Vol. 29 ›› Issue (3): 151-156.DOI: 10.12016/j.issn.2096-1456.2021.03.002
• Basic Study • Previous Articles Next Articles
WANG Chenwei1(),SUN Fangfang1,YANG Chuncheng2,DING Ling1,CHEN Xi1,ZHANG Jiaqi1,WU Guofeng1(
)
Received:
2020-07-05
Revised:
2020-08-03
Online:
2021-03-20
Published:
2021-01-12
Contact:
Guofeng WU
Supported by:
王琛玮1(),孙方方1,杨春成2,丁玲1,陈晞1,张嘉琪1,吴国锋1(
)
通讯作者:
吴国锋
作者简介:
王琛玮,住院医师,硕士研究生在读,Emai:基金资助:
WANG Chenwei,SUN Fangfang,YANG Chuncheng,DING Ling,CHEN Xi,ZHANG Jiaqi,WU Guofeng. Effects of concentrated sulfuric acid etching durations on the shear bond strength between polyether-ketone-ketone and dentin[J]. Journal of Prevention and Treatment for Stomatological Diseases, 2021, 29(3): 151-156.
王琛玮,孙方方,杨春成,丁玲,陈晞,张嘉琪,吴国锋. 浓硫酸酸蚀聚醚酮酮的时间对其与牙本质剪切粘接强度的影响[J]. 口腔疾病防治, 2021, 29(3): 151-156.
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Figure 1 Cross-sectional scanning electron microscopy images of PEKK after different concentrated sulfuric acid etching durations a: A group, there is no pore structure in the section, the cutting lines are clear and regular, and the whole is relatively flat; b: B group, the section has a spongy structure, and pore size is uniform; c: C group, pore size is not uniform, the number of pores decreases gradually, and a small amount of porous collapse occurs; d: D group, large amount of disintegration exists in the pore; A: control group, no etching treatment with concentrated sulfuric acid; B: etched by 98% concentrated sulfuric acid for 5 s; C: etched by 98% concentrated sulfuric acid for 30 s; D: etched by 98% concentrated sulfuric acid for 60 s; PEKK: polyether-ketone-ketone
Figure 2 Comparison of shear bond strengths between PEKK and dentin after different concentrated sulfuric acid etching durations *: vs. A group, P<0.05; A: control group, no etching treatment with concentrated sulfuric acid; B: etched by 98% concentrated sulfuric acid for 5 s; C: etched by 98% concentrated sulfuric acid for 30 s; D: etched by 98% concentrated sulfuric acid for 60 s; PEKK: polyether-ketone-ketone
Groups | Adhesive cement/dentin | Adhesive cement/PEKK | Cohesive in dentin | Cohesive in PEKK | Mixed |
---|---|---|---|---|---|
A | 0 | 10 | 0 | 0 | 0 |
B | 0 | 0 | 0 | 1 | 9 |
C | 0 | 4 | 0 | 0 | 6 |
D | 0 | 8 | 0 | 0 | 2 |
Table 1 The bonding failure types after different concentrated sulfuric acid etching durations
Groups | Adhesive cement/dentin | Adhesive cement/PEKK | Cohesive in dentin | Cohesive in PEKK | Mixed |
---|---|---|---|---|---|
A | 0 | 10 | 0 | 0 | 0 |
B | 0 | 0 | 0 | 1 | 9 |
C | 0 | 4 | 0 | 0 | 6 |
D | 0 | 8 | 0 | 0 | 2 |
Figure 3 Scanning electron microscopy images of bonding failure types after different concentrated sulfuric acid etching durations a: A group, the fracture surface is relatively flat without residual attachment; b: B group, the fracture surface is protruding with a large amount of residual attachments; c: C group, the fracture surface is slightly depressed and has a large number of corrosion-like structures; d: D group, the fracture surface is slightly depressed and has a large number of corrosion-like structures, the surface has less residual attachment than that of group C; A: control group, no etching treatment with concentrated sulfuric acid; B: etched by 98% concentrated sulfuric acid for 5 s; C: etched by 98% concentrated sulfuric acid for 30 s; D: etched by 98% concentrated sulfuric acid for 60 s; PEKK: polyether-ketone-ketone
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